Cavendish prepared hydrogen in 1766 by the novel method of passing steam through a red-hot gun barrel:
4H2O (g) + 3Fe (s) ⟶Fe3O4 (s) + 4H2 (g) 4H2O (g) + 3Fe (s) ⟶Fe3O4 (s) + 4H2 (g)
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